R&D 100 Award-Winning Technology for Drugs of Abuse |
Recommended Use Optimized phase deactivated to improve inertness, peak shape, and quantitation for drug compounds |
Agilent® | Restek® | SGE® |
---|---|---|
DB®-1ms DB-5ms DB-35 |
Rtx®-1ms Rtx®-5 Rtx-5ms Rtx-35ms |
SPB®-1 |
Column:
As listed.
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Dimension:
10 meter x 0.18 mm x 0.18 µm
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Injection:
Split 10:1 @ 360 °C, 1 µL*
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Carrier Gas:
Helium @ 1.2 mL/min (constant flow)
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Oven Program:
140 °C to 320 °C @ 20 °C for 1 min
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Detection:
MSD @ 230 °C
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Sample:
Analytes @ 10 ppm BSTFA/Pyridine
1. Codeine-d6 2. Codeine 3. Morphine-d3 4. Morphine |
Column:
As listed.
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Dimension:
10 meter x 0.18 mm x 0.18 µm
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Part No.:
7CD-G023-08
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Injection:
Split 10:1 @ 280 °C, 1 µL
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Carrier Gas:
Helium @ 55 cm/sec (constant flow)
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Oven Program:
180 °C to 340 °C @ 20 °C/min
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Detection:
MSD @ 230 °C
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Sample:
Analytes @ 10 ppm BSTFA/Pyridine
1. Codeine-d6 2. Codeine 3. Morphine-d3 4. Morphine |
Columns:
Zebron ZB-Drug-1
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Dimension:
10 meter x 0.18 mm x 0.18 μm
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Part No.:
7CD-G023-08
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Injection:
Split 10:1 @ 260 °C,1 μL
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Carrier Gas:
Helium @ 1 mL/min (constant flow)
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Oven Program:
50 ºC to 150 ºC @ 15 ºC/min to 240 ºC @ 7 ºC/min to 320 ºC @ 25 ºC/min for 2 min
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Detector:
MSD @ 320 °C; 45-450 amu |
Sample:
Analytes are 25 ppm in Methanol 1. Acetophenone 2. Nicotine 3. Benzocaine 4. Ibuprofen 5. Allobarbital 6. Aprobarbital 7. Butalbital 8. Amobarbital 9. Phenacetin 10. Pentobarbital 11. Acetaminophen 12. Benzphetamine 13. Secobarbital 14. Phencyclidine 15. Meprobamate 16. Diphenhydramine 17. Lidocaine 18. Hexobarbital 19. Doxylamine 20. Glutethimide 21. Caffeine |
22. Chlorpheniramine 23. Methapyrilene 24. Phenobarbital 25. Procaine 26. Methadone 27. Bromopheniramine 28. Propoxyphene 29. Trimipramine 30. Chlorcyclizine 31. Cocaine 32. Desipramine 33. Codeine 34. Morphine 35. Diazepam 36. Hydrocodone 37. 6-MAM 38. Oxymorphone 39. Heroin 40. Fentanyl 41. Ibogaine 42. Triazolam 43. LSD |