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Determination of Pesticide Residues in Kale and Grapes using QuEChERS and LC-MS/MS (TN-0115)
Following the EN 15662 pesticide residue method using roQ™ QuEChERS extraction and clean-up dSPE kits, along with the use of a highly efficient and broad polarity Kinetex ® 5 μm Biphenyl Core-Shell HPLC column, a pesticide screening method was developed using LC-MS/MS in under 16 minutes. Over 200 pesticides were screened at concentration ranges between 0.01 ppm to 1 ppm with the majority of analytes having a recovery range of 70-130 %. The method produced excellent selectivity and reproducibility for the earlier eluting polar pesticides owing to the use of QuEChERS for removing sample matrix interferences and the biphenyl bonded-phase chemistry of the Kinetex Biphenyl column for the chromatographic separation across the entire range of pesticides.
Determination of Pesticide Residues in Kale and Grapes using QuEChERS and LC-MS/MS (TN-0115)
Following the EN 15662 pesticide residue method using roQ™ QuEChERS extraction and clean-up dSPE kits, along with the use of a highly efficient and broad polarity Kinetex ® 5 μm Biphenyl Core-Shell HPLC column, a pesticide screening method was developed using LC-MS/MS in under 16 minutes. Over 200 pesticides were screened at concentration ranges between 0.01 ppm to 1 ppm with the majority of analytes having a recovery range of 70-130 %. The method produced excellent selectivity and reproducibility for the earlier eluting polar pesticides owing to the use of QuEChERS for removing sample matrix interferences and the biphenyl bonded-phase chemistry of the Kinetex Biphenyl column for the chromatographic separation across the entire range of pesticides.
Document Type:
Technical Notes
Target Industries:
Techniques:
Brands:
Separation Modes:
QuEChERS, Reversed Phase
Phases:
Determination of Pesticide Residues in Kale and Grapes using QuEChERS and LC-MS/MS (TN-0115)
Following the EN 15662 pesticide residue method using roQ™ QuEChERS extraction and clean-up dSPE kits, along with the use of a highly efficient and broad polarity Kinetex ® 5 μm Biphenyl Core-Shell HPLC column, a pesticide screening method was developed using LC-MS/MS in under 16 minutes. Over 200 pesticides were screened at concentration ranges between 0.01 ppm to 1 ppm with the majority of analytes having a recovery range of 70-130 %. The method produced excellent selectivity and reproducibility for the earlier eluting polar pesticides owing to the use of QuEChERS for removing sample matrix interferences and the biphenyl bonded-phase chemistry of the Kinetex Biphenyl column for the chromatographic separation across the entire range of pesticides.
| Target Industries: | Food Testing. Food Safety & Food Quality Analysis. |
| Techniques: | HPLC, HPLC Reversed Phase, QuEChERS, Sample Preparation |
| Brands: | Kinetex, SecurityGuard, roQ QuEChERS Kit |
| Separation Modes: | QuEChERS, Reversed Phase |
| Phases: | Kinetex Biphenyl |
Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide
Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide