Recommended Use
Herbicides/Insecticides, PCBs, Pesticides, Unknown Samples
Column:
Zebron ZB-XLB-HT Inferno
|
Dimension:
30 meter x 0.25 mm x 0.25 µm
|
Part No.:
7HG-G024-11
|
Injection:
Split 2:1 @ 250 °C, 1 µL, pressure pulse
@ 40 psi for first 0.25 min
|
Carrier:
Helium @ 1.5 mL/min (constant flow)
|
Oven Program:
50 °C for 0.5 min to 210 °C @ 40 °C/min
for 3 min to 230 °C @ 30 °C/min for 5 min
to 250 °C @ 30 °C/min for 5 min to 320 °C @ 40 °C/min for 2 min |
Detection:
ECD @ 350 °C |
Sample:
Total concentration of aroclors was
90 ppm in isooctane1. TCMX 2. BZ# 31 3. BZ# 28 4. BZ# 52 5. BZ# 101 6. BZ# 77 7. BZ# 123 8. BZ# 118 9. BZ# 153 10. BZ# 114 11. BZ# 105 12. BZ# 138 13. BZ# 126 14. BZ# 167 15. BZ# 156 16. BZ# 180 17. BZ# 157 18. BZ# 170 19. BZ# 169 20. BZ# 189 21. DCB |
Columns:
Zebron ZB-XLB-HT Inferno
|
Dimension:
15 meter x 0.25 mm x 0.25 µm
|
Part No.:
7EG-G024-11
|
Injection:
On-Column @ 103 °C, 1 µL
|
Carrier Gas:
Helium @ 1.4 mL/min (constant flow)
|
Oven Program:
100 °C for 0.5 min to 320 °C @ 25 °C/min
|
Detector:
MSD @ 325 °C |
Sample:
Analytes are 200 ng / 100 µL in
BSTFA / Pyridine (1:1)1. Cyanuric Acid 13C3 (IS) 2. Cyanuric Acid 3. Melamine 13C3 15N3 (IS) 4. Melamine |
Columns:
Zebron ZB-XLB-HT Inferno
|
Dimension:
15 meter x 0.25 mm x 0.25 µm
|
Part No.:
7EG-G024-11
|
Injection:
On-Column @ 73 °C, 0.5 µL
|
Carrier Gas:
Helium @ 1.4 mL/min (constant flow)
|
Oven Program:
70 °C for 1 min to 140 °C @ 25 °C/min
for 4 min to 280 °C @ 25 °C/min
|
Detector:
MSD @ 325 °C |
Sample:
Analytes are 10 ppm in dichloromethane1. Nitrobenzene 2. 2-Nitrotoluene 3. 3-Nitrotoluene 4. 4-Nitrotoluene 5. Nitroglycerin 6. 2,6-Dinitrotoluene (2,6-DNT) 7. 1,3-Dinitrobenzene (1,3-DNB) 8. 2,4-Dinitrotoluene 9. 2,4,6-Trinitrotoluene (2,4,6-TNT) 10. PETN 11. 1,3,5-Trinitrobenzene (1,3,5-TNB 12. RDX 13. 4-Amino-2,6-dinitrotoluene 14. 3,5-Nitroaniline 15. 2-Amino-4,6-dinitrotoluene 16. Tetryl |