Recommended Use
Amines, Aroclors, Chemicals, Drugs, EPA Methods (508, 608, 8081, 8141, 8151), Pesticides, Pharmaceuticals, Semi-volatiles, Steroids
R&D 100 Award-Winning |
Recommended Use Intermediate polarity with high temperature stability (up to 400 °C) for high boilers, contaminants, carry-overs, and high-temp bakeouts |
Agilent® | Restek® | SGE® | Supelco® | OV® |
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DB®-35 |
Rtx®-35 Rtx-35ms |
BPX35 BPX608 |
MDN-35 SPB®-35 SPB-608 |
OV-11 |
Dimension:
30 meter x 0.25 mm x 0.25 μm
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Injection:
Split 20:1 @ 200 °C, 1 µL
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Carrier Gas:
Helium @ 1.7 mL/min (constant flow)
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Oven Program:
100 °C to 320 °C @ 30 °C/min for 5 min to
340 °C @ 20 °C/min for 5 min to 360 °C @ 20 °C/min for 5 min to 380 °C @ 20 °C/min for 5 min to 400 °C @ 20 °C/min for 5 min to 100 °C @ 30 °C/min for 8 min |
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Detector:
FID @ 405 °C
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Part No.:
7HG-G025-11 (ZB-35HT Inferno)
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Injection:
A) Split 50:1 @ 350 °C, 1 µL
B) Split 50:1 @ 300 °C, 1 µL |
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Carrier Gas:
Helium @ 2.1 mL/min (constant flow)
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Oven Program:
A) 140 °C to 400 °C @ 10 °C/min
B) 140 °C to 300 °C @ 10 °C/min |
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Detector:
A) FID @ 400 °C
B) FID @ 320 °C |
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Sample:
1. Hexadecylamine
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Note:
Chromatogram is courtesy of
Northeastern Chemical Company.
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Column:
Zebron ZB-35 Inferno
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Dimension:
30 meter x 0.25 mm x 0.25 µm
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Part No.:
7HG-G025-11
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Injection:
Splitless @ 265 °C, 2 µL
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Carrier Gas:
Helium @ 1 mL/min (constant flow)
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Oven Program:
85 °C for 3 min to 320 °C @ 7 °C /min
for 8 min |
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Detector:
MSD @ 280 °C |
Sample:
Compounds are 5 ppm 1. Naphthalene 2. Acenaphthylene 3. Acenaphthene 4. Fluorene 5. Phenanthrene 6. Anthracene 7. PCB 28 8. PCB 52 9. PCB 101 10. Fluoranthene 11. Pyrene |
Sample:
12. PCB 118 13. PCB 153 14. PCB 138 15. PCB 180 16. Benz[a]anthracene 17. Chrysene 18. PCB 194 19. Benzo[b]fluoranthene 20. Benzo[k]fluoranthene 21. Benzo[a]pyrene 22. Indeno[1,2,3-cd]pyrene 23. Dibenz[a,h]anthracene 24. Benzo[g,h,I]perylene |