| 1C16:0 |
|---|
| 2C18:1 cis 9 |
| 3C18:2 cis 9,12 |
| 4C18:3 cis 9,12,15 |
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Applications
FAMEs In Walnut Oil by GC/MS on Zebron ZB-FAME
24075
Separation Mode: Application Specific
Application Specific
ZB-FAME
GC
Enzyme Inhibitors
Food & Beverage
Analytes
Details
GC Conditions (App ID: 24075)
Column: |
Part No: |
Phase Name: ZB-FAME |
Sample Notes: Recommended Accessories:
Recommended Liner: Zebron PLUS Single Taper Z-Liner, 4 mm ID
Liner Part No.: AG2-0A13-05 (for Agilent systems)
Inlet Seal: AG0-8620 (Gold Plated Easy Seal)
Septum: AG0-4696 (PhenoRed-400)
Sample Preparation:
1. Weigh out 25 mg of oil into a 5 mL screw cap glass vial
2. Add 2 mL of BF3-methanol to sample vial
3. Heat vial at 60 °C for 15 minutes with periodic vortexing
4. Remove from heat and allow to attain room temperature
5. Add 1 mL water followed by 1 mL hexane
6. Vortex for 1 minute
7. Remove upper organic layer
8. Dry hexane layer over anhydrous sodium sulfate
9. Transfer to autosampler vial and inject on GC |
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Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide