| 1C11:0 (I.S.) |
|---|
| 2C16:0 |
| 3C16:1 cis 9 |
| 4C18:0 |
| 5C18:1 cis 9 |
| 6C18:2 cis 9,12 |
| 7C18:3 cis 9,12,15 |
| 8C20:0 |
| 9C20:1 cis 11 |
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Applications
FAMEs In Regular Olive Oil by GC/FID on Zebron ZB-FAME (60 m)
23926
Separation Mode: Application Specific
Application Specific
ZB-FAME
GC
Enzyme Inhibitors
Food & Beverage
Analytes
Details
GC Conditions (App ID: 23926)
Column: |
Part No: |
Phase Name: ZB-FAME |
Sample Notes: Recommended Liner: Zebron PLUS Single Taper with Wool, 4 mm ID
Liner Part No.: AG2-0A11-05 (for Agilent systems)
Inlet Seal: AG0-8620 (Gold Plated Easy Seal)
Septum: AG0-4696 (PhenoRed-400)
Sample Preparation:
1. Strata® Si-1 Tube, 1 g/6 mL (Part No.: 8B-S012-JCH) on a vacuum or positive pressure manifold
2. Wash cartridge with 6 mL of hexane
3. Load oil solution (0.12 g of oil in 0.5 mL of hexane)
4. Elute with 10 mL of hexane/diethyl ether (87:13)
5. Evaporate eluate under a steady stream of nitrogen
6. Dissolve purified oil residue in 1mL of heptane
7. Add 0.1 mL of 2N potassium hydroxide in methanol to purified oil solution
8. Cap tube and shake vigorously for 15 seconds
9. Leave to separate until upper layer becomes clear
10. Extract upper layer for GC analysis |
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Phenomenex is a technology leader committed to developing novel analytical chemistry solutions that solve the separation and purification challenges of researchers worldwide