1Cyanuric acid |
---|
2Cyanuric-13C3 |
1Cyanuric acid |
---|
2Cyanuric-13C3 |
Column: |
Brand Name: Luna |
Part No: |
Phase Name: HILIC |
Sample Note: LC/MS/MS Condition:
Column: Luna 3µm HILIC, 100x2.0mm; Flow rate: 0.4ml/min
Mobile Phase: Isocratic; 90/10 ACN/100mM NH4 Formate pH 3.2; MS Detector: API 3000 LC/MS/MS with ESI (TurboIonSpray®) (www.Appliedbiosystems.com), Switch from -ve Ion Mode (for cyanuric) to Positive Ion (for Melamine);
MRM; heater gas flow 7000 cc/min; heater temperature 450 °C
Cyanuric acid QC - 200 ng
% Accuracy 100.1%
% CV 17%
Calibration Curve of Extracted Samples
conc. (ng) % Accuracy
20 104%
40 98%
200 95%
400 103%
2000 99.91% |