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Applications
Analysis of Phenylbutazone on Kinetex 2.6u XB-C18 50x2.1 by LC-MS-MS API 4000
21871
Separation Mode: Reversed Phase
Reversed Phase
XB-C18
HPLC
Anti-Inflammatory Agents, Non-Steroidal
Food & Beverage

Applications

Analysis of Phenylbutazone on Kinetex 2.6u XB-C18 50x2.1 by LC-MS-MS API 4000
Analytes
1Phenylbutazone
2Phenylbutazone-d10
3impurity
Compound Name
Phenylbutazone
CID
4781
Molecular Formula
C19H20N2O2
Molecular Weight
308
No. Hydrogen Bond Acceptors
2
Details
LC Conditions (App ID: 21871)
Column:
Brand Name:
Kinetex
Part No:
Phase Name:
XB-C18
Elution Type:
Gradient
Mobile Phase:
A: 0.1% Formic Acid in DI Water
B: 0.1% Formic Acid in Methanol
Gradient Profile:
Step No.Time(min)%A%B
105050
20.55050
32595
43.5595
53.515050
655050
Flow Rate:
0.45 mL/min
Temperature:
45°C
Detection:
Mass Spectrometer (MS)
Detector Info:
SCIEX API 4000
Sample Note:
Mass spec conditions: API 4000, ESI TurboIon Spray, + Ionization; CAD: 6.00 CUR: 20.00 GS1: 50.00 GS2: 50.00 IS: 5500.00 TEM: 600.00 ihe: ON DP 50.00 EP 10.00

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