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75 °C for 1 min to 320 °C @ 15 °C/min for 2.67 min.
Carrier Gas:
Constant Flow Helium, 0.9 mL/min
Detection:
Mass Selective (MSD) (320°C)
Sample Notes:
Low Concentration Spiked Sample of Baby Formula using Scan Mode.
Analytes were extracted via Liqiud/Liquid Extraction (LLE) method, centrifuged, filtered, and deriviatized with BSTFA in pyridine as per FDA Screening Method.
Cyanuric Acid (345*, 330, 188)
Melamine (327*, 342, 197)
Ammelide (344*, 329, 198)
Ammeline (328*, 343, 285)
DACP [IS] (273*, 288, 237)