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Applications
Organochloropesticides (OCP) and Polychlorinated Biphenyls (PCB) in Milk and Milk Products by GC/ECD
17909
Separation Mode: Application Specific
Application Specific
ZB-MultiResidue-1
GC
Insecticides
Food & Beverage
Pesticide / Insecticide
Environmental / Health

Applications

Organochloropesticides (OCP) and Polychlorinated Biphenyls (PCB) in Milk and Milk Products by GC/ECD
Analytes
1alpha-HCH
2Hexachlorobenzene
3gamma-HCH
4beta-HCH
5delta-HCH
6PCB 28
7PCB 52
8Aldrin
9Heptachloro epoxide
102,4'-DDE (o,p-)
11PCB 101
124,4'-DDE (p,p-)
13Nitrofen
14Dieldrin
152,4'-DDD (o,p-)
16Endrin
174,4'-DDD (p,p-)
18PCB 153
19PCB 138
20PCB 180
21Mirex
Compound Name
Lindane
CID
727
Molecular Formula
C6H6Cl6
Molecular Weight
290
Details
GC Conditions (App ID: 17909)
Column:
Part No:
Phase Name:
ZB-MultiResidue-1
Injection:
Splitless @ 50°C, 5.0 μL
Oven Program:
100 °C for 2 min, with 30 °C/min to 160 °C, with 2 °C/min to 170 °C, with 4 °C/min to 190°C and 10 min hold, with 10 °C/min to 220 °C and 5 min hold, with 10 °C/min to 250°C and 5 min hold
Carrier Gas:
Constant Flow Hydrogen, 1.5 mL/min
System:
Agilent (HP) 6890
Detection:
Electron Capture (ECD) (300°C)
Sample Notes:
The application was kindly provided by the MLF, Dr.-Oskar-Farny-Institute in Wangen, Germany. Injector Gerstel-KAS3. Program: 50 °C with 12 °C/s to 300 °C, 3 min hold Solvent Venting Purge Time: 0.15 min, Splitless Time: 1 min, Equilibration Time 0.5 min, Initial Time: 0.15 min. Concentration: 25 ppb each for OCP + PCB, 100 ppb for Nitrofen

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